Carbamic chloride, N-methyl-N-phenyl- → HCID 10285903, compound

HRID 1831163Notes

Reaction equation

HRID 1831163 reaction equation
[OH:1][N:2]1[CH:6]=[CH:5][N:4]=[N:3]1.[CH3:7][N:8]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[C:9](Cl)=[O:10]>CCOC(C)=O.CCCCCCC>[N:2]1([O:1][C:9](=[O:10])[N:8]([CH3:7])[C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:6]=[CH:5][N:4]=[N:3]1

Participants

4

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 10877052HCID 10877052, compound

Product 1

HCID 10285903HCID 10285903, compound

Reagents, catalysts & solvents 1

HCID 21899848Ethylacetate heptaneSolvent

Procedure

The title compound was prepared from 1-hydroxy-1,2,3-triazole and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to flash chromatography (Quad flash 25, EtOAc-heptane) (80%, oil). HPLC-MS m/z=219.1 (M+1), Rt: 2.50 min. Mp 105–106° C.

Sources & evidence

ORD record
ord-7dbf645205404fda8c30cf1baf267fb9
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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