Carbamic chloride, N-methyl-N-phenyl- → HCID 69519103, compound

HRID 1831165Notes

Reaction equation

HRID 1831165 reaction equation
[CH3:1][N:2]1[C:6]([CH3:7])=[C:5]([CH2:8][C:9]2[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=2)[C:4]([CH3:16])=[N:3]1.[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[CH3:1][N:2]1[C:6]([CH3:7])=[C:5]([CH2:8][C:9]2[CH:14]=[CH:13][C:12]([O:15][C:19](=[O:20])[N:18]([CH3:17])[C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)=[CH:11][CH:10]=2)[C:4]([CH3:16])=[N:3]1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 27637284-[(1,3,5-Trimethyl-1H-pyrazol-4-yl)methyl]phenol

Product 1

HCID 69519103HCID 69519103, compound

Procedure

The title product was prepared from 4-[(1,3,5-trimethyl-1H-pyrazol-4-yl)methyl]phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (88%, oil). HPLC-MS: m/z=350.0 (M+1); Rt: 3.52 min. (66% purity).

Sources & evidence

ORD record
ord-47f8f356141340c2bf2d62e391983472
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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