HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic acid 4-(2-cyano-ethyl)-phenyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Reactant | 3-(p-Hydroxyphenyl)propiononitrile | HCID 87079 | — |
| Product | Methyl-phenyl-carbamic acid 4-(2-cyano-ethyl)-phenyl ester | HCID 69519626 | — |
Reaction Steps
The title product was prepared from 3-(4-hydroxyphenyl)proprionitrile and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (11%, colourless oil). HPLC-MS: m/z=281.2 (M+1); Rt: 3.75 min, purity 80%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-273e6fb17d244c03afc826be6eea6c5c |
| Source note | uspto-grants-2006_06 |