Carbamic chloride, N-methyl-N-phenyl- → HCID 69519353, compound

HRID 1831167Notes

Reaction equation

HRID 1831167 reaction equation
[S:1]1[C:5]([NH:6][C:7]2[CH:12]=[CH:11][C:10]([OH:13])=[CH:9][CH:8]=2)=[N:4][N:3]=[N:2]1.[CH3:14][N:15]([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:16](Cl)=[O:17]>>[S:1]1[C:5]([NH:6][C:7]2[CH:8]=[CH:9][C:10]([O:13][C:16](=[O:17])[N:15]([CH3:14])[C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)=[CH:11][CH:12]=2)=[N:4][N:3]=[N:2]1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 90174p-(1,2,3,4-thiatriazol-5-ylamino)phenol

Product 1

HCID 69519353HCID 69519353, compound

Procedure

The title product was prepared from 4-(1,2,3,4-thiatriazol-5-ylamino)phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (10%, light brown solid material). HPLC-MS: m/z=328.0 (M+1); Rt: 3.69 min, purity 81%.

Sources & evidence

ORD record
ord-2228519dc6584924a9f11c309f9eaa41
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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