HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-5-hydroxypyridine → Methyl-phenyl-carbamic Acid 6-methyl-pyridin-3-yl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-5-hydroxypyridine | HCID 14275 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | Methyl-phenyl-carbamic Acid 6-methyl-pyridin-3-yl Ester | HCID 69518367 | — |
Reaction Steps
The title product was prepared from 3-hydroxy-6-methyl-pyridine and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (79%, colourless oil). HPLC-MS: m/z=243.1 (M+1); Rt: 2.24 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-ea11e214c79b41018280acd50cf25ce3 |
| Source note | uspto-grants-2006_06 |