Carbamic chloride, N-methyl-N-phenyl- → HCID 69465809, compound

HRID 1831181Notes

Reaction equation

HRID 1831181 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][N:3]=1.[CH3:8][N:9]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:10](Cl)=[O:11]>>[N:3]1[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=1[O:1][C:10](=[O:11])[N:9]([CH3:8])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 178516071HCID 178516071, compound

Product 1

HCID 69465809HCID 69465809, compound

Procedure

The title product was prepared from 2-hydroxypyridine and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC. (57%, colorless oil). HPLC-MS: m/z=229.1 (M+23); Rt: 2.80 min.

Sources & evidence

ORD record
ord-e9a6153bbee34e6899ed0dc7f3e73398
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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