HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxyacetanilide → HCID 69518100, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxyacetanilide | HCID 12124 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | HCID 69518100 | HCID 69518100 | — |
Reaction Steps
The title product was prepared from 3-acetamidophenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (66%, white solid). HPLC-MS: m/z=285.1 (M+1); Rt: 3.09 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-f6a5639869a1455b8d3882da5d8aaef3 |
| Source note | uspto-grants-2006_06 |