HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,6,7,8-Tetrahydro-1-naphthol → Methyl-phenyl-carbamic Acid 5,6,7,8-tetrahydro-naphthalen-1-yl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,6,7,8-Tetrahydro-1-naphthol | HCID 68258 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | Methyl-phenyl-carbamic Acid 5,6,7,8-tetrahydro-naphthalen-1-yl Ester | HCID 69518203 | — |
Reaction Steps
The title product was prepared from 5,6,7,8-tetrahydro-1-naphthol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (42%, colorless oil). HPLC-MS: m/z=282.1 (M+1); Rt: 4.77 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-5d3ae5f0a2f848e4a51a94cdf0da64e3 |
| Source note | uspto-grants-2006_06 |