Carbamic chloride, N-methyl-N-phenyl- → HCID 23635399, compound

HRID 1831196Notes

Reaction equation

HRID 1831196 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:8][C:9]2[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=2)=[N:6][CH:7]=1.[CH3:16][N:17]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:18](Cl)=[O:19]>C(OCC)(=O)C.CCCCCCC>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:8][C:9]2[CH:14]=[CH:13][C:12]([O:15][C:18](=[O:19])[N:17]([CH3:16])[C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)=[CH:11][CH:10]=2)=[N:6][CH:7]=1

Participants

4

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 21655016HCID 21655016, compound

Product 1

HCID 23635399HCID 23635399, compound

Reagents, catalysts & solvents 1

HCID 21899848Ethylacetate heptaneSolvent

Procedure

The title product was prepared from 4-(5-chloro-pyridin-2-yloxy)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to column chromatography (ethyl acetate/heptane (1:5) (85%, white solid). HPLC-MS: m/z=355.1 (M+1); Rt: 4.56 min.

Sources & evidence

ORD record
ord-6ec960eea5ce43d8ab4cec45cd2a4e32
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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