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HRID1831198

反应详情

EQUATION

反应方程式

HRID 1831198 的结构方程式

REACTANTS

反应物

2
结构：CN(C(=O)Cl)c1ccccc1
HCID77969

Carbamic chloride, methylphenyl-

C8H8ClNO

结构：Oc1ccc(N2CCOCC2)cc1
HCID80510

4-Morpholinophenol

C10H13NO2

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(N2CCOCC2)cc1)c1ccccc1
HCID10171887

未命名化合物

PROCEDURE

实验过程

The title product was prepared from and 4-morpholin-4-yl-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was extracted with dichloromethane from citric acid (5%). The combined organic phases were evaporated and the product crystallized from ethanol (22%, crystals). HPLC-MS: m/z=313.2 (M+1); Rt: 3.75 min.

WORKUP

后处理

  1. extractionThe crude product was extracted with dichloromethane from citric acid (5%)
  2. customThe combined organic phases were evaporated
  3. customthe product crystallized from ethanol (22%, crystals)