Carbamic chloride, N-methyl-N-phenyl- → HCID 69520198, compound

HRID 1831201Notes

Reaction equation

HRID 1831201 reaction equation
[Cl:1][C:2]1[CH:16]=[CH:15][C:5]([CH2:6][CH2:7][C:8]2[CH:13]=[CH:12][C:11]([OH:14])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][CH2:7][C:8]2[CH:13]=[CH:12][C:11]([O:14][C:19](=[O:20])[N:18]([CH3:17])[C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)=[CH:10][CH:9]=2)=[CH:15][CH:16]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 1490307HCID 1490307, compound

Product 1

HCID 69520198HCID 69520198, compound

Procedure

The title product was prepared from 4-(4-chlorophenethyl)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (57%, white crystals). HPLC-MS: m/z=366.1 (M+1); Rt: 5.58 min.

Sources & evidence

ORD record
ord-1068f480a37546168a42b6219003ee66
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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