HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic chloride, N-methyl-N-phenyl- → Methyl-phenyl-carbamic Acid 4-[(pyridine-2-carbonyl)-amino]-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Reactant | HCID 11356337 | HCID 11356337 | — |
| Product | Methyl-phenyl-carbamic Acid 4-[(pyridine-2-carbonyl)-amino]-phenyl Ester | HCID 10215434 | — |
Reaction Steps
The title product was prepared from pyridine-2-carboxylic acid (4-hydroxy-phenyl)-amide and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (41%,). HPLC-MS: m/z=348.1 (M+1); Rt: 4.00 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-b6edb0acd33c462f8a63d7e467697515 |
| Source note | uspto-grants-2006_06 |