HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 4-hydroxyphenyl ketone → Methyl-phenyl-carbamic Acid 4-phenylacetyl-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 4-hydroxyphenyl ketone | HCID 75607 | — |
| Reactant | Carbamic chloride, N-methyl-N-phenyl- | HCID 77969 | — |
| Product | Methyl-phenyl-carbamic Acid 4-phenylacetyl-phenyl Ester | HCID 69518528 | — |
Reaction Steps
The title product was prepared from benzyl 4-hydroxyphenyl ketone and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (68%, light yellow oil). HPLC-MS: m/z=431.2 (M+1); Rt: 3.55 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-003301af047944049c847ea369739124 |
| Source note | uspto-grants-2006_06 |