Bis(4-hydroxyphenyl)methane → HCID 69519171, compound

HRID 1831211Notes

Reaction equation

HRID 1831211 reaction equation
[CH:1]1[C:6]([CH2:7][C:8]2[CH:9]=[CH:10][C:11]([OH:14])=[CH:12][CH:13]=2)=[CH:5][CH:4]=[C:3]([OH:15])[CH:2]=1.[CH3:16][N:17]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:18](Cl)=[O:19]>>[OH:15][C:3]1[CH:2]=[CH:1][C:6]([CH2:7][C:8]2[CH:13]=[CH:12][C:11]([O:14][C:18](=[O:19])[N:17]([CH3:16])[C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)=[CH:10][CH:9]=2)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 12111Bis(4-hydroxyphenyl)methaneHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 69519171HCID 69519171, compound

Procedure

The title compound was prepared from 4,4′-dihydroxydiphenylmethane and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to preparative HPLC (21%, white crystals which turn red after standing). HPLC-MS: m/z=324.2 (M+1); Rt: 4.21 min.

Sources & evidence

ORD record
ord-6bd5f5dee98f4b3a9023d7f501926b2e
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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