HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofurfurylamine → Methyl-phenyl-carbamic Acid 4-[(tetrahydro-furan-2-ylmethyl)-carbamoyl]-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofurfurylamine | HCID 253298 | — |
| Reactant | 4-(Methyl-phenyl-carbamoyloxy)-benzoic Acid 2,5-dioxo-pyrrolidin-1-yl Ester | HCID 86589206 | — |
| Product | Methyl-phenyl-carbamic Acid 4-[(tetrahydro-furan-2-ylmethyl)-carbamoyl]-phenyl Ester | HCID 69517656 | — |
Reaction Steps
The title product was prepared from 4-(methyl-phenyl-carbamoyloxy)-benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester and C-(tetrahydro-furan-2-yl)methylamine. The crude product was used without further purification (86%, oil). HPLC-MS: m/z=(M+1); Rt: min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-0ffe9ac5511e432a9dc83e34d63d8969 |
| Source note | uspto-grants-2006_06 |