1-Hydroxybenzotriazole → HCID 86589207, compound

HRID 1831265Notes

Reaction equation

HRID 1831265 reaction equation
[OH:1][N:2]1[C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[N:4]=[N:3]1.[CH3:11][N:12]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[C:13](Cl)=[O:14]>>[N:2]1([O:1][C:13](=[O:14])[N:12]([CH3:11])[C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[N:4]=[N:3]1

Participants

3

Reactant 2

HCID 757711-HydroxybenzotriazoleHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 86589207HCID 86589207, compound

Procedure

The title compound was prepared from 1-hydroxybenzotriazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (98%, crystallizes slowly).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (98%
  2. customcrystallizes slowly)

Sources & evidence

ORD record
ord-cfa91e0e152346969f1f8ebad0681625
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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