Carbamic chloride, N-methyl-N-phenyl- → HCID 10193467, compound

HRID 1831268Notes

Reaction equation

HRID 1831268 reaction equation
[OH:1][N:2]1[CH:6]=[CH:5][C:4]([C:7]2[CH:12]=[CH:11][C:10]([N+:13]([O-:15])=[O:14])=[CH:9][CH:8]=2)=[N:3]1.[CH3:16][N:17]([C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=1)[C:18](Cl)=[O:19]>>[N+:13]([C:10]1[CH:9]=[CH:8][C:7]([C:4]2[CH:5]=[CH:6][N:2]([O:1][C:18](=[O:19])[N:17]([CH3:16])[C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)[N:3]=2)=[CH:12][CH:11]=1)([O-:15])=[O:14]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 10954693HCID 10954693, compound

Product 1

HCID 10193467HCID 10193467, compound

Procedure

The title compound was prepared from 1-hydroxy-3-(4-nitrophenyl)pyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (99%, yellow crystals).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (99%, yellow crystals)

Sources & evidence

ORD record
ord-93be2ec9e51442b889700d4302710e77
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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