Carbamic chloride, N-methyl-N-phenyl- → HCID 10171758, compound

HRID 1831270Notes

Reaction equation

HRID 1831270 reaction equation
[OH:1][N:2]1[CH:6]=[CH:5][C:4]([C:7]2[S:8][CH:9]=[CH:10][CH:11]=2)=[N:3]1.[CH3:12][N:13]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[C:14](Cl)=[O:15]>>[S:8]1[CH:9]=[CH:10][CH:11]=[C:7]1[C:4]1[CH:5]=[CH:6][N:2]([O:1][C:14](=[O:15])[N:13]([CH3:12])[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[N:3]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 10942807HCID 10942807, compound

Product 1

HCID 10171758HCID 10171758, compound

Procedure

The title compound was prepared from 1-hydroxy-3-(2-thienyl)pyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (66%, oil).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (66%, oil)

Sources & evidence

ORD record
ord-c30a85444b654510b4ccbf4bae7f42cf
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

Loading…