Carbamic chloride, N-methyl-N-phenyl- → HCID 69518141, compound

HRID 1831279Notes

Reaction equation

HRID 1831279 reaction equation
[OH:1][N:2]1[C:6]([I:7])=[C:5]([I:8])[CH:4]=[N:3]1.[CH3:9][N:10]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[C:11](Cl)=[O:12]>>[I:8][C:5]1[CH:4]=[N:3][N:2]([O:1][C:11](=[O:12])[N:10]([CH3:9])[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[C:6]=1[I:7]

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 22047748HCID 22047748, compound

Product 1

HCID 69518141HCID 69518141, compound

Procedure

The title compound was prepared from 1-hydroxy-4,5-diiodopyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (76%, crystals).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (76%, crystals)

Sources & evidence

ORD record
ord-257e24531e604d7b9c7d5dfebf004d2d
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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