Carbamic chloride, N-methyl-N-phenyl- → HCID 10308409, compound

HRID 1831280Notes

Reaction equation

HRID 1831280 reaction equation
[OH:1][N:2]1[C:6]([C:7]2[S:8][CH:9]=[CH:10][CH:11]=2)=[CH:5][CH:4]=[N:3]1.[CH3:12][N:13]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[C:14](Cl)=[O:15]>>[S:8]1[CH:9]=[CH:10][CH:11]=[C:7]1[C:6]1[N:2]([O:1][C:14](=[O:15])[N:13]([CH3:12])[C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[N:3]=[CH:4][CH:5]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 22047933HCID 22047933, compound

Product 1

HCID 10308409HCID 10308409, compound

Procedure

The title compound was prepared from 1-hydroxy-5-(2-thienyl)pyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (51%, crystals).

Workup

  1. customThe crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (51%, crystals)

Sources & evidence

ORD record
ord-21c80c1601bd4be7a72aa1d6ec1e56b7
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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