HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Morpholinecarbonyl chloride → Morpholine-4-carboxylic Acid imidazol-1-yl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Morpholinecarbonyl chloride | HCID 84810 | — |
| Reactant | 1-Hydroxyimidazole | HCID 3614351 | — |
| Product | Morpholine-4-carboxylic Acid imidazol-1-yl Ester | HCID 45091617 | — |
Reaction Steps
The title compound was prepared from 1-hydroxyimidazole and 4-morpholine carbonyl chloride applying the general procedure 8. The crude product was purified by preparative HPLC (water-acetonitrile-0. 1% TFA) (36%, crystals).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-b9f1e68d25f7478eb3d9e458d95698d1 |
| Source note | uspto-grants-2006_06 |