Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-(Cyclopropylmethyl)piperazine → 4-Cyclopropylmethyl-piperazine-1-Carboxylic acid 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-(Cyclopropylmethyl)piperazine | HCID 965875 | — |
| 반응물 | 4-(4,4-Dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl chloroformate | HCID 22047895 | — |
| 생성물 | 4-Cyclopropylmethyl-piperazine-1-Carboxylic acid 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl Ester | HCID 57455846 | — |
반응 단계
The title compound was prepared from 4-(4,4-dimethyl-2,6-dioxo-piperidin-1-yl)-phenyl chloroformate and 1-cyclopropylmethyl-piperazine, preparative HPLC (Method C) (45%, off-white crystals). HPLC-MS m/z=400.3 (M+1), Rt: 1.83 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07067517B2 |
| 출처 데이터셋 | uspto-grants-2006_06 |
| ORD ID | ord-cd417f03f9fc4ca8b0c2aa7ceabbf32f |
| 출처 메모 | uspto-grants-2006_06 |