HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorothiophene-2-boronic acid → HCID 69519597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorothiophene-2-boronic acid | HCID 2734324 | — |
| Reactant | Methyl-phenyl-carbamic Acid 4-iodo-phenyl Ester | HCID 69517304 | — |
| Product | HCID 69519597 | HCID 69519597 | — |
Reaction Steps
The title compound was prepared from methyl-phenyl-carbamic acid 4-iodo-phenyl ester and 5-chloro-2-thiopheneboronic acid. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane 1:9) (53%, pink crystals).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-6823645782364687aff7add4508a9bcf |
| Source note | uspto-grants-2006_06 |