Succinimide → HCID 69518519, compound

HRID 1831439Notes

Reaction equation

HRID 1831439 reaction equation
O[CH2:2][CH2:3][C:4]1[CH:9]=[CH:8][C:7]([O:10][C:11](=[O:20])[N:12]([CH3:19])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:6][CH:5]=1.[C:21]1(=[O:27])[NH:25][C:24](=[O:26])[CH2:23][CH2:22]1>>[O:26]=[C:24]1[CH2:23][CH2:22][C:21](=[O:27])[N:25]1[CH2:2][CH2:3][C:4]1[CH:9]=[CH:8][C:7]([O:10][C:11](=[O:20])[N:12]([CH3:19])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 11439SuccinimideHCID 69520342Methyl-phenyl-carbamic Acid 4-(2-hydroxy-ethyl)-phenyl Ester

Product 1

HCID 69518519HCID 69518519, compoundYield 85%

Procedure

The title compound was prepared in 85% yield as crystals using methyl-phenyl-carbamic acid 4-(2-hydroxy-ethyl)-phenyl ester and succinimide. 1H NMR (400 MHz; CDCl3): δ 2.65 (s, 4H), 2.86 (t, 2H), 3.41 (br s, 3H), 3.72 (t, 2H), 7.04 (br d, 2H), 7.19 (d, 2H), 7.26–7.42 (m, 5H); HPLC-MS: m/z=353.2 (M+1); Rt=3.17 min.

Sources & evidence

ORD record
ord-8914ee9c08964894bbcf2f7ab65f1d3e
Source dataset
uspto-grants-2006_06
Patent number
US07067517B2

Reaction notes

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