HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl-phenyl-carbamic Acid 4-hydroxymethyl-phenyl Ester → Methyl-phenyl-carbamic Acid 4-tetrazol-1-ylmethyl-phenyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl-phenyl-carbamic Acid 4-hydroxymethyl-phenyl Ester | HCID 69518671 | — |
| Reactant | HCID 178418441 | HCID 178418441 | — |
| Product | Methyl-phenyl-carbamic Acid 4-tetrazol-1-ylmethyl-phenyl Ester | HCID 69520746 | 6% |
Reaction Steps
The title compound was prepared in 6% yield as an oil using methyl-phenyl-carbamic acid 4-hydroxymethyl-phenyl ester and tetrazole. 1H NMR (400 MHz; CDCl3): δ 3.42 (br s, 3H), 5.57 (s, 2H), 7.17 (br s, 2H), 7.26–7.42 (m, 7H), 8.52 (s, 1H); HPLC-MS: m/z=332.0 (M+23); Rt=3.24 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067517B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-2ca4c8af5ec74995b928e4f8b9dd7a21 |
| Source note | uspto-grants-2006_06 |