2-Pentanamine → [4-(2,4-Dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methyl-butyl)-amine

Participants

Role	Name	HCID	Charge
Reactant	2-Pentanamine	HCID 12246	—
Reactant	2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine	HCID 22052102	—
Product	[4-(2,4-Dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methyl-butyl)-amine	HCID 22052043	87%

Reaction Steps

2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine (0.20 g, 0.66 mmol) and 1-methyl-butylamine (0.11 g, 1.32 mmol) were treated substantially as described in Part D of Example 9 to produce 0.20 g (87%) of crude [4-(2,4-dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1-methyl-butyl)-amine: MS (AP) m/z 354.2 [(M+H)+, 100].

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07067658B2
Source dataset	uspto-grants-2006_06
ORD ID	ord-995d45a089e14ff49da4dcbea1423842
Source note	uspto-grants-2006_06