HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Cyclopropylpropan-1-amine → (1-Cyclopropyl-propyl)-[4-(2,4-dichloro-phenyl)-3-nitro-pyridin-2-yl]-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Cyclopropylpropan-1-amine | HCID 3985879 | — |
| Reactant | 2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine | HCID 22052102 | — |
| Product | (1-Cyclopropyl-propyl)-[4-(2,4-dichloro-phenyl)-3-nitro-pyridin-2-yl]-amine | HCID 11057630 | 736.6% |
Reaction Steps
2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine (0.26 g, 0.86 mmol) and 1-cyclopropyl-propylamine (0.23 g, 1.71 mmol) were substantially as described in Part D of Example 9 to produce 2.32 g (100%) of crude (1-cyclopropyl-propyl)-[4-(2,4-dichloro-phenyl)-3-nitro-pyridin-2-yl]-amine: MS (AP) m/z 366.2 [(M+H)+, 96].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067658B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-3041f4fad30d4cb6884c428ca8a6a2f6 |
| Source note | uspto-grants-2006_06 |