HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dimethylpropylamine → HCID 22052121, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dimethylpropylamine | HCID 11731 | — |
| Reactant | 2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine | HCID 22052102 | — |
| Product | HCID 22052121 | HCID 22052121 | 111.2% |
Reaction Steps
2-Chloro-4-(2,4-dichloro-phenyl)-3-nitro-pyridine (0.20 g, 0.66 mmol) and 1,2-dimethyl-propylamine (0.11 g, 1.32 mmol) were treated substantially as described in Part D of Example 9 to produce 0.26 g (100%) of [4-(2,4-dichloro-phenyl)-3-nitro-pyridin-2-yl]-(1,2-dimethyl-propyl)-amine. MS (AP) m/z 354.2 [(M+H)+, 100].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067658B2 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-195bce5346514f33b3a2924091ecda1f |
| Source note | uspto-grants-2006_06 |