Stannous Chloride → HCID 69658372, compound

Participants

Reaction Steps

[4-(2-Chloro-5-fluoro-4-methoxy-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine (35 mg, 0.09 mmol) and SnCl2 (51 mg, 0.27 mmol) were treated substantially as described in Part D of Example 74a to yield 30 mg (94%) of 4-(2-Chloro-5-fluoro-4-methoxy-phenyl)-N2-(1-methoxymethyl-propyl)-pyridine-2,3-diamine: MS (EI) m/z 354.22 [(M+H)+, 100].

Provenance & Evidence