HCID 22052227, compound → HCID 69658055, compound

Participants

Reaction Steps

[4-(2-Chloro-4-dimethylamino-5-fluoro-phenyl)-3-nitro-pyridin-2-yl]-(1-methoxymethyl-propyl)-amine (30.0 mg, 0.076 mmol) and SnCl2.H2O (43.2 mg, 0.23 mmol) were treated substantially as described in Part D of Example 74a to yield 30 mg (100% crude) of 4-(2-Chloro-4-dimethylamino-5-fluoro-phenyl)-N2-(1-methoxymethyl-propyl)-pyridine-2,3-diamine: MS (EI) m/z 367.23 [(M+H)+, 100].

Provenance & Evidence