HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 69587603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 86584324 | HCID 86584324 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69587603 | HCID 69587603 | — |
Reaction Steps
A mixture of 4-[4-(1-Ethyl-propylamino)-3,6-dimethyl-pyridin-2-yloxy]-3,5-dimethyl-benzaldehyde and sodium borohydride in methanol was stirred at room temperature. After standard work-up procedure and purification, the title compound was obtained as a solid. 1H NMR(CDCl3) d 7.06(s,2H), 6.08(s,1H), 4.64(s,2H), 3.74(d,1H), 3.33(m,1H), 2.14(s,3H), 2.13(s,3H), 2.11(s,6H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067664B1 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-06d8114d67de4d718d557a29a5061c43 |
| Source note | uspto-grants-2006_06 |