HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22291309, compound → HCID 21912039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22291309 | HCID 22291309 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21912039 | HCID 21912039 | — |
Reaction Steps
The title compound was prepared by reacting of 2-{4-[4-(1-Ethyl-propylamino)-3,6-dimethyl-pyridin-2-yloxy]-3,5-dimethyl-phenyl}-propan-2-ol with Burgess Inner salt (Et3NS(O)2NCOOMe in benzene at reflux for 30 min. 1H NMR(CDCl3) d 7.17(s,2H), 6.08(s,1H), 5.34(s,1H), 5.02(s,1H), 3.72(d,1H), 3.32(m,1H), 2.12 and 2.15 (two sets of s, 12H), 1.4–1.6(m,4H), 0.97(t,6H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067664B1 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-d98aa2eb8d9c453991967876648159cf |
| Source note | uspto-grants-2006_06 |