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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1831676Generated: October 30, 2026

HCID 22291309, compound → HCID 21912039, compound

https://huagongshe.com/reaction/1831676

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22291309HCID 22291309—
SolventBenzeneHCID 241—
ProductHCID 21912039HCID 21912039—

Reaction Steps

The title compound was prepared by reacting of 2-{4-[4-(1-Ethyl-propylamino)-3,6-dimethyl-pyridin-2-yloxy]-3,5-dimethyl-phenyl}-propan-2-ol with Burgess Inner salt (Et3NS(O)2NCOOMe in benzene at reflux for 30 min. 1H NMR(CDCl3) d 7.17(s,2H), 6.08(s,1H), 5.34(s,1H), 5.02(s,1H), 3.72(d,1H), 3.32(m,1H), 2.12 and 2.15 (two sets of s, 12H), 1.4–1.6(m,4H), 0.97(t,6H) ppm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07067664B1
Source datasetuspto-grants-2006_06
ORD IDord-d98aa2eb8d9c453991967876648159cf
Source noteuspto-grants-2006_06