HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 21912061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | Boron Trichloride | HCID 25135 | — |
| Reactant | HCID 21912418 | HCID 21912418 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21912061 | HCID 21912061 | — |
Reaction Steps
The title compound was prepared by reacting 1-[2-(4-Chloro-2,6-dimethyl-phenoxy)-3-methoxy-6-methyl-pyridin-4-yl]-2-ethyl-butan-1-one with BBr3 or BCl3 in THF or methylene chloride. 1H NMR (CDCl3) d 7.04(s,2H), 7.01(s,1H), 3.26(m,1H), 2.24(s,3H), 2.08(s,6H), 1.80(m,2H), 1.63(m,2H), 0.91(t,6H) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067664B1 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-de1899a23a994ca9b355230710a1d7f4 |
| Source note | uspto-grants-2006_06 |