HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21912303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Reactant | HCID 21912102 | HCID 21912102 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21912303 | HCID 21912303 | — |
Reaction Steps
The title compound was prepared by reacting 4-(1-ethyl-propoxy)-6-methyl-N2-(2,4,6-trimethyl-phenyl)-pyridine-2,3-diamine with triphosgene, NEt3 in THF at room temperature. A white solid was isolated, mp. 184–186° C. Anal. For C21H27N3O2 calc. C, 71.36; H, 7.70; N, 11.89; found: C, 71.09; H, 7.75; N, 11.63.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067664B1 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-b16cabd493dc496a8351b4aba37d38f7 |
| Source note | uspto-grants-2006_06 |