HCID 21912454, compound → HCID 69587609, compound

HRID 1831720Notes

Reaction equation

HRID 1831720 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([CH3:8])[N:5]=[C:4]([O:9][C:10]2[C:15]([CH3:16])=[CH:14][C:13]([CH3:17])=[CH:12][C:11]=2[CH3:18])[C:3]=1[CH2:19]Cl.[C:21]([O:28][CH3:29])(=[O:27])[CH2:22][C:23]([O:25][CH3:26])=[O:24].[H-].[Na+]>CO>[CH3:26][O:25][C:23](=[O:24])[CH:22]([CH2:19][C:3]1[C:4]([O:9][C:10]2[C:15]([CH3:16])=[CH:14][C:13]([CH3:17])=[CH:12][C:11]=2[CH3:18])=[N:5][C:6]([CH3:8])=[CH:7][C:2]=1[Cl:1])[C:21]([O:28][CH3:29])=[O:27]

Participants

4

Reactant 2

HCID 21912454HCID 21912454, compoundHCID 86584335HCID 86584335, compound

Product 1

HCID 69587609HCID 69587609, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The title compound was prepared by reacting 4-chloro-3-chloromethyl-6-methyl-2-(2,4,6-trimethyl-phenoxy)-pyridine with dimethyl malonate/NaH in methanol. The title compound was isolated as a colorless oil.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-ba53a611c82b48aab9b1fd87b4859641
Source dataset
uspto-grants-2006_06
Patent number
US07067664B1

Reaction notes

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