2,2-dimethyl-3,4-dihydro-2H-1-benzopyran-6-carbaldehyde → HCID 22049447, compound

HRID 1832389Notes

Reaction equation

HRID 1832389 reaction equation
[CH3:1][C:2]1([CH3:14])[CH2:11][CH2:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([CH:12]=O)[CH:8]=2)[O:3]1.[CH3:15][CH:16]([CH3:32])[C:17]([NH:19][C:20]1[CH:25]=[CH:24][CH:23]=[C:22]([CH:26]2[CH2:31][CH2:30][NH:29][CH2:28][CH2:27]2)[CH:21]=1)=[O:18]>>[CH3:1][C:2]1([CH3:14])[CH2:11][CH2:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([CH2:12][N:29]3[CH2:30][CH2:31][CH:26]([C:22]4[CH:21]=[C:20]([NH:19][C:17](=[O:18])[CH:16]([CH3:15])[CH3:32])[CH:25]=[CH:24][CH:23]=4)[CH2:27][CH2:28]3)[CH:8]=2)[O:3]1

Participants

3

Reactant 2

HCID 17977512,2-dimethyl-3,4-dihydro-2H-1-benzopyran-6-carbaldehydeHCID 167572552-methyl-N-[3-(4-piperidyl)phenyl]propanamide

Product 1

HCID 22049447HCID 22049447, compound

Procedure

Prepared by Procedure F and Scheme R using 2,2-dimethyl-6-chromanecarbaldehyde and 2-methyl-N-[3-(4-piperidinyl)phenyl]propanamide: ESMS m/e: 421.2 (M+H)+.

Workup

  1. customPrepared by Procedure F and Scheme R

Sources & evidence

ORD record
ord-4718f1c9354947bcaf225cda0a9462af
Source dataset
uspto-grants-2006_06
Patent number
US07067534B1

Reaction notes

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