4-[(4-methylphenyl)sulfanyl]-3-nitrobenzaldehyde → HCID 22048630, compound

HRID 1832413Notes

Reaction equation

HRID 1832413 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[CH:16]=[CH:15][C:12]([CH:13]=O)=[CH:11][C:10]=2[N+:17]([O-:19])=[O:18])=[CH:4][CH:3]=1.[CH3:20][CH:21]([CH3:37])[C:22]([NH:24][C:25]1[CH:30]=[CH:29][CH:28]=[C:27]([CH:31]2[CH2:36][CH2:35][NH:34][CH2:33][CH2:32]2)[CH:26]=1)=[O:23]>>[CH3:20][CH:21]([CH3:37])[C:22]([NH:24][C:25]1[CH:30]=[CH:29][CH:28]=[C:27]([CH:31]2[CH2:36][CH2:35][N:34]([CH2:13][C:12]3[CH:15]=[CH:16][C:9]([S:8][C:5]4[CH:6]=[CH:7][C:2]([CH3:1])=[CH:3][CH:4]=4)=[C:10]([N+:17]([O-:19])=[O:18])[CH:11]=3)[CH2:33][CH2:32]2)[CH:26]=1)=[O:23]

Participants

3

Reactant 2

HCID 7358484-[(4-methylphenyl)sulfanyl]-3-nitrobenzaldehydeHCID 167572552-methyl-N-[3-(4-piperidyl)phenyl]propanamide

Product 1

HCID 22048630HCID 22048630, compound

Procedure

Prepared by Procedure F and Scheme R using 4-[(4-methylphenyl)sulfanyl]-3-nitrobenzaldehyde and 2-methyl-N-[3-(4-piperidinyl)phenyl]propanamide: ESMS m/e: 504.2 (M+H)+.

Workup

  1. customPrepared by Procedure F and Scheme R

Sources & evidence

ORD record
ord-16a1170ff99f433d9219f5a4762562eb
Source dataset
uspto-grants-2006_06
Patent number
US07067534B1

Reaction notes

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