4-(Trifluoromethoxy)phenylhydrazine hydrochloride → HCID 22049277, compound

HRID 1832607Notes

Reaction equation

HRID 1832607 reaction equation
O1CCO[CH:2]1[CH2:6][CH2:7][CH2:8][N:9]1[CH2:14][CH2:13][CH:12]([C:15]2[CH:16]=[C:17]([NH:21][C:22](=[O:26])[CH:23]([CH3:25])[CH3:24])[CH:18]=[CH:19][CH:20]=2)[CH2:11][CH2:10]1.Cl.[F:28][C:29]([F:40])([F:39])[O:30][C:31]1[CH:36]=[CH:35][C:34]([NH:37]N)=[CH:33][CH:32]=1>>[CH3:24][CH:23]([CH3:25])[C:22]([NH:21][C:17]1[CH:18]=[CH:19][CH:20]=[C:15]([CH:12]2[CH2:11][CH2:10][N:9]([CH2:8][CH2:7][C:6]3[C:35]4[C:34](=[CH:33][CH:32]=[C:31]([O:30][C:29]([F:40])([F:39])[F:28])[CH:36]=4)[NH:37][CH:2]=3)[CH2:14][CH2:13]2)[CH:16]=1)=[O:26]

Participants

3

Reactant 2

HCID 27773284-(Trifluoromethoxy)phenylhydrazine hydrochlorideHCID 22048812HCID 22048812, compound

Product 1

HCID 22049277HCID 22049277, compound

Procedure

Prepared by Procedure H and Scheme S using N-(3-{1-[3-(1,3-dioxolan-2-yl)propyl]-4-piperidinyl}phenyl)-2-methylpropanamide and 1-[4-(trifluoromethoxy)phenyl]hydrazine hydrochloride: ESMS m/e: 474.2 (M+H)+.

Workup

  1. customPrepared by Procedure H and Scheme S

Sources & evidence

ORD record
ord-9b06c7d852574360b49d4e61c65d0f42
Source dataset
uspto-grants-2006_06
Patent number
US07067534B1

Reaction notes

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