4-(Trifluoromethoxy)phenylhydrazine hydrochloride → HCID 22049579, compound

HRID 1832611Notes

Reaction equation

HRID 1832611 reaction equation
O1CCO[CH:2]1[CH2:6][CH2:7][CH2:8][CH2:9][N:10]1[CH2:15][CH2:14][CH:13]([C:16]2[CH:17]=[C:18]([NH:22][C:23](=[O:27])[CH:24]([CH3:26])[CH3:25])[CH:19]=[CH:20][CH:21]=2)[CH2:12][CH2:11]1.Cl.[F:29][C:30]([F:41])([F:40])[O:31][C:32]1[CH:37]=[CH:36][C:35]([NH:38]N)=[CH:34][CH:33]=1>>[CH3:25][CH:24]([CH3:26])[C:23]([NH:22][C:18]1[CH:19]=[CH:20][CH:21]=[C:16]([CH:13]2[CH2:12][CH2:11][N:10]([CH2:9][CH2:8][CH2:7][C:6]3[C:36]4[C:35](=[CH:34][CH:33]=[C:32]([O:31][C:30]([F:41])([F:40])[F:29])[CH:37]=4)[NH:38][CH:2]=3)[CH2:15][CH2:14]2)[CH:17]=1)=[O:27]

Participants

3

Reactant 2

HCID 27773284-(Trifluoromethoxy)phenylhydrazine hydrochlorideHCID 22048802N-(3-{1-[4-(1,3-dioxolan-2-yl)butyl]4-piperidinyl}phenyl)-2-methylpropanamide

Product 1

HCID 22049579HCID 22049579, compound

Procedure

Prepared by Procedure H and Scheme S using N-(3-{1-[4-(1,3-dioxolan-2-yl)butyl]-4-piperidinyl}phenyl)-2-methylpropanamide and 1-[4-(trifluoromethoxy)phenyl]hydrazine hydrochloride: ESMS m/e: 488.2 (M+H)+.

Workup

  1. customPrepared by Procedure H and Scheme S

Sources & evidence

ORD record
ord-a5c316b0f5414f338893806d6f1a4b52
Source dataset
uspto-grants-2006_06
Patent number
US07067534B1

Reaction notes

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