4-(Trifluoromethoxy)phenylhydrazine hydrochloride → HCID 22049133, compound

HRID 1832929Notes

Reaction equation

HRID 1832929 reaction equation
[CH3:1][CH:2]([CH3:33])[C:3]([NH:5][C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]2[CH2:17][CH2:16][N:15]([CH2:18][CH2:19][CH2:20][CH2:21][C:22]([C:24]3[CH:29]=[CH:28][CH:27]=[C:26]([N+:30]([O-:32])=[O:31])[CH:25]=3)=O)[CH2:14][CH2:13]2)[CH:7]=1)=[O:4].Cl.[F:35][C:36]([F:47])([F:46])[O:37][C:38]1[CH:43]=[CH:42][C:41]([NH:44]N)=[CH:40][CH:39]=1>>[CH3:1][CH:2]([CH3:33])[C:3]([NH:5][C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([CH:12]2[CH2:13][CH2:14][N:15]([CH2:18][CH2:19][CH2:20][C:21]3[C:42]4[C:41](=[CH:40][CH:39]=[C:38]([O:37][C:36]([F:35])([F:46])[F:47])[CH:43]=4)[NH:44][C:22]=3[C:24]3[CH:29]=[CH:28][CH:27]=[C:26]([N+:30]([O-:32])=[O:31])[CH:25]=3)[CH2:16][CH2:17]2)[CH:7]=1)=[O:4]

Participants

3

Reactant 2

HCID 27773284-(Trifluoromethoxy)phenylhydrazine hydrochlorideHCID 22048907HCID 22048907, compound

Product 1

HCID 22049133HCID 22049133, compound

Procedure

Prepared by Procedure E and Scheme M using 2-methyl-N-(3-{1-[5-(3-nitrophenyl)-5-oxopentyl]-4-piperidinyl}phenyl)propanamide and 4-(trifluoromethoxy)phenylhydrazine hydrochloride: ESMS m/e: 609.1 (M+H)+.

Workup

  1. customPrepared by Procedure E and Scheme M

Sources & evidence

ORD record
ord-ba64dad9df8f4577b3cabe6000f3f844
Source dataset
uspto-grants-2006_06
Patent number
US07067534B1

Reaction notes

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