HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 22049115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-methyl-N-[3-(4-piperidyl)phenyl]propanamide | HCID 16757255 | — |
| Reactant | 7-Chloro-1-(2-fluorophenyl)heptan-1-one | HCID 22048584 | — |
| Product | HCID 22049115 | HCID 22049115 | — |
Reaction Steps
Prepared by Procedure K and Scheme E using K2CO3 instead of Na2CO3 and NaI instead of KI and 7-chloro-1-(2-fluorophenyl)-1-heptanone and 2-methyl-N-[3-(4-piperidinyl)phenyl]propanamide: 1H NMR (400 MHz, CDCl3), δ 8.17 (s, br, 1H), 8.06–6.88 (m, 8H), 3.08–2.94 (m, 4H), 2.62–2.48 (m, 1H), 2.48–2.38 (m, 1H), 2.38–2.15 (m, 2H), 2.02–1.92 (m, 2H), 1.84–1.77 (m, 4H), 1.77–1.66 (m, 2H), 1.62–1.46 (m, 2H), 1.46–1.29 (M, 4H), 1.21 (d, 6H, J=6.8 Hz); ESMS m/e: 453.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07067534B1 |
| Source dataset | uspto-grants-2006_06 |
| ORD ID | ord-2412d46e494943ff884a5a7f2a1630e5 |
| Source note | uspto-grants-2006_06 |