Hydrochloric Acid → HCID 22048845, compound

Participants

Reaction Steps

Prepared by Procedure A and Scheme AN using 1-(3-hydroxyphenyl)ethanone and N-(3-{1-[5-(4-chlorophenyl)-5-hydroxypentyl]-4-piperidinyl}phenyl)-2-methylpropanamide: 1H NMR (400 MHz, CDCl3), HCl salt δ 8.05 (s, br, 1H), 7.74–6.88 (m, 12H), 5.27–5.16 (m, 1H), 3.69–3.52 (m, br, 2H), 3.10–2.81 (br, 2H), 2.81–2.57 (m, br, 4H), 2.54 (s, 3H), 2.52–2.40 (m, br, 2H), 2.05–1.80 (m, br, 6H), 1.66–1.42 (m, br, 2H), 1.25 (d, 6H, J=6.8 Hz); Anal. Calc. for C34H42Cl2N2O30.5CH2Cl2.1.0H2O: C, 63.46; H, 6.91; N, 4.30. Found: C, 63.46; H, 7.09; N, 4.00. ESMS m/e: 561.1 (M+H)+.

Provenance & Evidence