HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 54161447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Methyl 3-(2-nitrophenoxy)-1H-indole-2-carboxylate | HCID 54304514 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54161447 | HCID 54161447 | — |
Reaction Steps
A mixture of 3.12g of methyl-3-[o-nitrophenoxy]-indole-2-carboxylate, 10g of 40 mesh iron filings, 5ml of 5% aqueous acetic acid and 300ml of ethanol was refluxed with stirring for 3 hours. The mixture was filtered and concentrated to a solid. Recrystallization from ethanol gave analytical material, mp. 183°-4°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04066660 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-5164e81c0f134ed5ae9afd1a5b2edfcf |
| Source note | uspto-grants-1978_01 |