Isopropylamine → HCID 637899, compound

HRID 1833412Notes

Reaction equation

HRID 1833412 reaction equation
[C:1]1(=O)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH:8]([NH2:11])([CH3:10])[CH3:9]>>[CH3:9][CH:8]([N:11]=[C:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)[CH3:10]

Participants

3

Reactant 2

HCID 6363IsopropylamineHCID 7967Cyclohexanone

Product 1

HCID 637899HCID 637899, compound

Procedure

To a mixture of 600 g. cyclohexanone and 1 l. isopropylamine are added 500 g. Linde Type 3A molecular sieves. The mixture is allowed to stand overnight at room temperature, after which the isopropylamine is removed in vacuo at room temperature. The oily residue is 1-methyl-N-(cyclohexylidene)-ethylamine.

Workup

  1. additionTo a mixture of 600 g
  2. customafter which the isopropylamine is removed in vacuo at room temperature

Sources & evidence

ORD record
ord-22a31fb30ade4b9eae3f733baf172b6c
Source dataset
uspto-grants-1978_01
Patent number
US04066665

Reaction notes

Loading…