HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54012549, compound → HCID 54328425, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54012549 | HCID 54012549 | — |
| Reactant | 2-(Hydroxyimino)-3,5,5-trimethyl-1,3-thiazolidin-4-one | HCID 71363389 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 54328425 | HCID 54328425 | — |
Reaction Steps
To a solution of 2.5g (0.015m) of 3,5,5-trimethyl-2-oximino-thiazolidin-4-one and 3.93g (0.015m) of N-methyl-N-(2-benzoyl-2-propanesulfenyl)carbamoyl chloride in 100 ml of dioxane was added 1.5g (0.015m) of triethylamine. After stirring at room temperature for 16 hours, the reaction mixture was diluted with water and the product isolated in ethylacetate. Recrystallized from isopropyl ether. Weight of the product 1.3g, m.p. 98°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04066689 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-50ab7a82ed724744a250a30257d03fb7 |
| Source note | uspto-grants-1978_01 |