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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1833627Erstellt: 25. Oktober 2026

3-((4-Chloro-2-nitrophenyl)amino)propan-1-ol → 3-((2-Amino-4-chlorophenyl)amino)propan-1-ol

https://huagongshe.com/reaction/1833627

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-((4-Chloro-2-nitrophenyl)amino)propan-1-olHCID 603976—
EduktHCID 178418361HCID 178418361—
LösungsmittelEthanolHCID 702—
Produkt3-((2-Amino-4-chlorophenyl)amino)propan-1-olHCID 3017357—

Reaktionsschritte

A mixture of 34.6 parts of 3-[(4-chloro-2-nitrophenyl)amino]-1-propanol and 320 parts of ethanol is hydrogenated at normal pressure and at room temperature with 8 parts of Raneynickel catalyst. After the calculated amount of hydrogen is taken up, the catalyst is filtered off and the filtrate is evaporated, yielding 30 parts of 3-[(2-amino-4-chlorophenyl)amino]-1-propanol as an oily residue.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04066772
Quelldatensatzuspto-grants-1978_01
ORD IDord-e3b0e547c36b45a4a9c3ed2100f46e34
Quellennotizuspto-grants-1978_01