HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-((4-Chloro-2-nitrophenyl)amino)propan-1-ol → 3-((2-Amino-4-chlorophenyl)amino)propan-1-ol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-((4-Chloro-2-nitrophenyl)amino)propan-1-ol | HCID 603976 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-((2-Amino-4-chlorophenyl)amino)propan-1-ol | HCID 3017357 | — |
Reaktionsschritte
A mixture of 34.6 parts of 3-[(4-chloro-2-nitrophenyl)amino]-1-propanol and 320 parts of ethanol is hydrogenated at normal pressure and at room temperature with 8 parts of Raneynickel catalyst. After the calculated amount of hydrogen is taken up, the catalyst is filtered off and the filtrate is evaporated, yielding 30 parts of 3-[(2-amino-4-chlorophenyl)amino]-1-propanol as an oily residue.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04066772 |
| Quelldatensatz | uspto-grants-1978_01 |
| ORD ID | ord-e3b0e547c36b45a4a9c3ed2100f46e34 |
| Quellennotiz | uspto-grants-1978_01 |