HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21388868, compound → 2-(4-Pentylphenyl)pyrimidine-5-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21388868 | HCID 21388868 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 2-(4-Pentylphenyl)pyrimidine-5-carbonitrile | HCID 13574824 | — |
Reaction Steps
6.3 G. of 4-chloro-5-cyano-2-(4-n-pentylphenyl)-pyrimidine are reacted in 290 ml. of 50% dioxane with 25.3 g. of pre-treated zinc dust and worked up after the reaction in a manner analogous to that described in Example 13. There is obtained 5-cyano-2-(4-n-pentylphenyl)-pyrimidine as colorless crystals having a melting point of 96.0°-96.2° C. and clearing point of 109.0° C. The substance is identical with the compound obtained according to Example
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04066570 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-8c7eecc8efec494fb092525d85f43c90 |
| Source note | uspto-grants-1978_01 |