Acetic Anhydride → 1-Chloro-4-acetoxynonane

HRID 1833754Notes

Reaction equation

HRID 1833754 reaction equation

[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([OH:11])[CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:12](OC(=O)C)(=[O:14])[CH3:13]>>[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([O:11][C:12](=[O:14])[CH3:13])[CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

3

Reactant 2

HCID 7918Acetic Anhydride

HCID 203860821-Chlorononan-4-ol

Product 1

HCID 131047161-Chloro-4-acetoxynonane

Procedure

A mixture of 1-chloro-4-nonanol (111.99 g.; 0.627 mole) and acetic anhydride (128.0 g.; 1.254 moles) is heated on a steam bath for 11/2 hours.

Workup

temperatureis heated on a steam bath for 11/2 hours

Sources & evidence

ORD record: ord-ebe73855201646c6a3f343545531658e
Source dataset: uspto-grants-1978_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04066692

Reaction notes

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