HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21387584, compound → HCID 21387534, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21387584 | HCID 21387584 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21387534 | HCID 21387534 | 87.6% |
Reaction Steps
A solution of 1-(2-ethylphenyl)-1-(2-furyl)ethylene (27 g.) in ethanol (150 ml.) in the presence of 10% palladium on charcoal (0.5 g.) was treated with hydrogen at room temperature for 3 hours. The mixture was filtered and evaporated to give a clear oil which was distilled to give (±) 2-[1-(2-ethylphenyl)ethyl]-furan (23.9 g.), b.p. 130°-150° C./20 mm.Hg, in the form of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04067723 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-9d9254fe7b88446b97d646546ae37c54 |
| Source note | uspto-grants-1978_01 |