HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-(phenylmethoxy)benzoate → Sodium 4-carboxyphenoxy phenyl methane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-(phenylmethoxy)benzoate | HCID 191414 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | Sodium 4-carboxyphenoxy phenyl methane | HCID 70551218 | — |
Reaction Steps
To a solution of 4-ethoxycarbonylphenoxy phenyl methane (6.3g) in ethanol (30ml), sodium hydroxide solution (70ml.; 10N) was added and the mixture boiled under reflux with vigorous stirring for 18 hr. After cooling the sodium salt was filtered off and dried, m.p. >340°
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04067892 |
| Source dataset | uspto-grants-1978_01 |
| ORD ID | ord-0a7d334a7ab04aeab1790d8fc36577fa |
| Source note | uspto-grants-1978_01 |